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dc.contributor.authorSerencam H.
dc.contributor.authorDuran C.
dc.contributor.authorOzdes D.
dc.contributor.authorBektas H.
dc.date.accessioned20.04.201910:49:12
dc.date.accessioned2019-04-20T21:44:25Z
dc.date.available20.04.201910:49:12
dc.date.available2019-04-20T21:44:25Z
dc.date.issued2013
dc.identifier.issn1318-0207
dc.identifier.urihttps://hdl.handle.net/20.500.12403/854
dc.description.abstractA simple and highly sensitive separation and preconcentration procedure, which has minimal impact on the environment, has been developed. The procedure is based on the carrier element free coprecipitation (CEFC) of Co(II), Cu(II), and Ni(II) ions by using 2-{4-[2-(1H-indol-3-yl)ethyl]-3-(4-methylbenzyl)-5-oxo- 4,5-dihydro-1H-1,2,4-triazol- 1-yl}-N'-(pyridin-2-yl methylidene)acetohydrazide (IMOTPA), as an organic coprecipitant. The levels of analyte ions were determined by flame atomic absorption spectrometry (FAAS). The detection limits for Co(II), Cu(II) and Ni(II) ions were found to be 0.40, 0.16 and 0.17 ?g L-1, respectively, and the relative standard deviations for the analyte ions were lower than 3.0%. Spike tests and certified reference material analyses were performed to validate the method. The method was successfully applied for the determination of Co(II), Cu(II) and Ni(II) ions levels in sea and stream water as liquid samples and red pepper, black pepper, and peppermint as solid samples.en_US
dc.language.isoengen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCarrier element free coprecipitation
dc.subjectFlame atomic absorption spectrometry
dc.subjectHeavy metals
dc.subjectPreconcentration
dc.subjectSeparation
dc.subjectcobalt
dc.subjectcopper
dc.subjectnickel
dc.subjectarticle
dc.subjectatomic absorption spectrometry
dc.subjectchemical model
dc.subjectfood contamination
dc.subjectlimit of detection
dc.subjectstandard
dc.subjectwater pollutant
dc.subjectCobalt
dc.subjectCopper
dc.subjectFood Contamination
dc.subjectLimit of Detection
dc.subjectModels, Chemical
dc.subjectNickel
dc.subjectReference Standards
dc.subjectSpectrophotometry, Atomic
dc.subjectWater Pollutants, Chemical
dc.subjectCarrier element free coprecipitation
dc.subjectFlame atomic absorption spectrometry
dc.subjectHeavy metals
dc.subjectPreconcentration
dc.subjectSeparation
dc.subjectcobalt
dc.subjectcopper
dc.subjectnickel
dc.subjectarticle
dc.subjectatomic absorption spectrometry
dc.subjectchemical model
dc.subjectfood contamination
dc.subjectlimit of detection
dc.subjectstandard
dc.subjectwater pollutant
dc.subjectCobalt
dc.subjectCopper
dc.subjectFood Contamination
dc.subjectLimit of Detection
dc.subjectModels, Chemical
dc.subjectNickel
dc.subjectReference Standards
dc.subjectSpectrophotometry, Atomic
dc.subjectWater Pollutants, Chemical
dc.titleApplication of carrier element free coprecipitation (CEFC) method for determination of Co(II), Cu(II) and Ni(II) ions in food and water samplesen_US
dc.typearticleen_US
dc.relation.journalActa Chimica Slovenicaen_US
dc.contributor.departmentBayburt Universityen_US
dc.contributor.authorID23100981600
dc.contributor.authorID16042074800
dc.contributor.authorID25646623400
dc.contributor.authorID14027930500
dc.identifier.volume60
dc.identifier.issue2
dc.identifier.startpage287
dc.identifier.endpage293
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US


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