Application of Carrier Element Free Coprecipitation (CEFC) Method for Determination of Co(II), Cu(II) and Ni(II) Ions in Food and Water Samples

dc.authoridDuran, Celal/0000-0002-1306-9061
dc.authoridOZDES, Duygu/0000-0002-8692-2676
dc.contributor.authorSerencam, Huseyin
dc.contributor.authorDuran, Celal
dc.contributor.authorOzdes, Duygu
dc.contributor.authorBektas, Hakan
dc.date.accessioned2024-10-04T18:48:18Z
dc.date.available2024-10-04T18:48:18Z
dc.date.issued2013
dc.departmentBayburt Üniversitesien_US
dc.description.abstractA simple and highly sensitive separation and preconcentration procedure, which has minimal impact on the environment, has been developed. The procedure is based on the carrier element free coprecipitation (CEFC) of Co(II), Cu(II), and Ni(II) ions by using 2-{4-[2-(1H-indol-3-yl)ethyl]-3-(4-methylbenzyl)-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl}-N'-(pyridin-2-yl methylidene)acetohydrazide (IMOTPA), as an organic coprecipitant. The levels of analyte ions were determined by flame atomic absorption spectrometry (FAAS). The detection limits for Co(II), Cu(II) and Ni(II) ions were found to be 0.40, 0.16 and 0.17 mu g L-1, respectively, and the relative standard deviations for the analyte ions were lower than 3.0%. Spike tests and certified reference material analyses were performed to validate the method. The method was successfully applied for the determination of Co(II), Cu(II) and Ni(II) ions levels in sea and stream water as liquid samples and red pepper, black pepper, and peppermint as solid samples.en_US
dc.description.sponsorshipUnit of the Scientific Research Projects of Karadeniz Technical University [1156]en_US
dc.description.sponsorshipAuthors wish to thank the Unit of the Scientific Research Projects of Karadeniz Technical University (Project No: 1156) for the financial support.en_US
dc.identifier.endpage293en_US
dc.identifier.issn1318-0207
dc.identifier.issn1580-3155
dc.identifier.issue2en_US
dc.identifier.pmid23878931en_US
dc.identifier.startpage287en_US
dc.identifier.urihttp://hdl.handle.net/20.500.12403/3007
dc.identifier.volume60en_US
dc.identifier.wosWOS:000322040900006en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherSlovensko Kemijsko Drustvoen_US
dc.relation.ispartofActa Chimica Slovenicaen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectHeavy metalsen_US
dc.subjectseparationen_US
dc.subjectpreconcentrationen_US
dc.subjectcarrier element free coprecipitationen_US
dc.subjectflame atomic absorption spectrometryen_US
dc.titleApplication of Carrier Element Free Coprecipitation (CEFC) Method for Determination of Co(II), Cu(II) and Ni(II) Ions in Food and Water Samplesen_US
dc.typeArticleen_US

Dosyalar