Simultaneous separation and preconcentration of Cd(II), Co(II), and Ni(II) ions in environmental samples by carrier element-free coprecipitation method prior to their flame atomic absorption spectrometric determination

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dc.authorid16042074800
dc.authorid25646623400
dc.authorid53876870600
dc.authorid23100981600
dc.authorid6602656875
dc.contributor.authorDuran C.
dc.contributor.authorOzdes D.
dc.contributor.authorAkcay H.T.
dc.contributor.authorSerencam H.
dc.contributor.authorTufekci M.
dc.date.accessioned20.04.201910:49:12
dc.date.accessioned2019-04-20T21:44:04Z
dc.date.available20.04.201910:49:12
dc.date.available2019-04-20T21:44:04Z
dc.date.issued2015
dc.departmentBayburt Üniversitesien_US
dc.description.abstractABSTRACT: In the present study, Cd(II), Co(II), and Ni(II) ions were separated and preconcentrated via carrier element-free coprecipitation (CEFC) method by using an organic coprecipitating agent, 1,2-bis-(2-tosyl ethoxy) benzene (BTEB), prior to their flame atomic absorption spectrometric (FAAS) detections. The experimental conditions were optimized in terms of pH of the aqueous solution, BTEB amount, standing time, centrifugation rate and time, and sample volume. Under the optimum experimental conditions, the detection limits for Cd(II), Co(II), and Ni(II) ions were found to be 0.13, 0.67, and 0.46 ?g L?1, respectively, and the relative standard deviations for the analyte ions were found to be lower than 4.0%. The accuracy of the method was tested by analyzing certified reference material and spike tests. The method was applied to determine the levels of Cd(II), Co(II), and Ni(II) ions in sea and stream water, macaroni, red lentil, and cracked wheat samples. © 2013, © 2013 Balaban Desalination Publications. All rights reserved.en_US
dc.identifier.doi10.1080/19443994.2013.839401
dc.identifier.endpage397
dc.identifier.issn1944-3994
dc.identifier.issue2
dc.identifier.scopus2-s2.0-84921026007en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage390
dc.identifier.urihttps://dx.doi.org/10.1080/19443994.2013.839401
dc.identifier.urihttps://hdl.handle.net/20.500.12403/761
dc.identifier.volume53
dc.identifier.wosWOS:000347687800013en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor and Francis Inc.
dc.relation.ispartofDesalination and Water Treatmenten_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCarrier element free coprecipitation
dc.subjectFlame atomic absorption spectrometry
dc.subjectHeavy metals
dc.subjectPreconcentration
dc.subjectSeparation
dc.subjectLens culinaris
dc.subjectTriticum aestivum
dc.subjectCarrier element free coprecipitation
dc.subjectFlame atomic absorption spectrometry
dc.subjectHeavy metals
dc.subjectPreconcentration
dc.subjectSeparation
dc.subjectLens culinaris
dc.subjectTriticum aestivum
dc.titleSimultaneous separation and preconcentration of Cd(II), Co(II), and Ni(II) ions in environmental samples by carrier element-free coprecipitation method prior to their flame atomic absorption spectrometric determinationen_US
dc.typeArticleen_US

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