Separation and pre-concentration of palladium(II) from environmental and industrial samples by formation of a derivative of 1,2,4-triazole complex on Amberlite XAD-2010 resin

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dc.authorid23100981600
dc.authorid16041213800
dc.authorid6602656875
dc.authorid16042269000
dc.authorid16042074800
dc.authorid55597972400
dc.authorid7006488616
dc.contributor.authorSerencam H.
dc.contributor.authorBulut V.N.
dc.contributor.authorTufekci M.
dc.contributor.authorGundogdu A.
dc.contributor.authorDuran C.
dc.contributor.authorHamza S.
dc.contributor.authorSoylak M.
dc.date.accessioned20.04.201910:49:12
dc.date.accessioned2019-04-20T21:44:29Z
dc.date.available20.04.201910:49:12
dc.date.available2019-04-20T21:44:29Z
dc.date.issued2013
dc.departmentBayburt Üniversitesien_US
dc.description.abstractA simple separation/pre-concentration method was developed for extraction of Pd(II) in various environmental samples, based on its adsorption of 4-phenyl-5-{[(4-phenyl-5-pyridin-4-yl-4H-1,2,4-triazole-3-yl)thio]methyl}-4H-1,2,4-triazole-3-thyol (PPTTMET) complex on Amberlite XAD-2010 resin in a mini column. The ligand has high affinity for Pd(II) among many other metals that are taken into consideration. The flame atomic absorption spectrometry is employed to determine the concentration of Pd(II). The optimum working conditions which were determined are as follows: 0.05 mol L-1 HNO3 as working medium, 1.0 mol L-1 HCI in acetone as elution solvent, 0.75 mg of PPTTMET amount and 750 mL of sample volume. The system was independent from the flow rates between 3.1 and 23.1 mL min-1. The Pd(II) adsorption capacity of Amberlite XAD-2010 resin was found to be 12.8 mg g-1 and the enrichment factor was calculated as 375. The method was successfully applied for the determination of Pd(II) in motorway dust samples, anodic sludge, gold ore, industrial electronic waste materials and various water samples. © 2013 Copyright Taylor and Francis Group, LLC.en_US
dc.identifier.doi10.1080/03067319.2012.755676
dc.identifier.endpage1499
dc.identifier.issn0306-7319
dc.identifier.issue14
dc.identifier.scopus2-s2.0-84890799664en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage1484
dc.identifier.urihttps://dx.doi.org/10.1080/03067319.2012.755676
dc.identifier.urihttps://hdl.handle.net/20.500.12403/868
dc.identifier.volume93
dc.identifier.wosWOS:000328602400003en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.relation.ispartofInternational Journal of Environmental Analytical Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subject4-phenly-5-{[(4-phenly-5-pyridyn-4-yl-4H-1,2,4-triazole-3-yl)thio]methyl}-4H-1,2,4-triazole-3-thyol
dc.subjectflame atomic absorption spectrometry
dc.subjectpalladium(II)
dc.subjectsolid phase extraction
dc.subject4-phenly-5-{[(4-phenly-5-pyridyn-4-yl-4H-1,2,4-triazole-3-yl)thio]methyl}-4H-1,2,4-triazole-3-thyol
dc.subjectAdsorption capacities
dc.subjectElectronic waste materials
dc.subjectEnvironmental sample
dc.subjectFlame atomic absorption spectrometry
dc.subjectIndustrial samples
dc.subjectOptimum working conditions
dc.subjectSolid-phase extraction
dc.subjectAcetone
dc.subjectAtomic absorption spectrometry
dc.subjectNitrogen compounds
dc.subjectOres
dc.subjectPalladium
dc.subjectResins
dc.subjectPalladium compounds
dc.subject4-phenly-5-{[(4-phenly-5-pyridyn-4-yl-4H-1,2,4-triazole-3-yl)thio]methyl}-4H-1,2,4-triazole-3-thyol
dc.subjectflame atomic absorption spectrometry
dc.subjectpalladium(II)
dc.subjectsolid phase extraction
dc.subject4-phenly-5-{[(4-phenly-5-pyridyn-4-yl-4H-1,2,4-triazole-3-yl)thio]methyl}-4H-1,2,4-triazole-3-thyol
dc.subjectAdsorption capacities
dc.subjectElectronic waste materials
dc.subjectEnvironmental sample
dc.subjectFlame atomic absorption spectrometry
dc.subjectIndustrial samples
dc.subjectOptimum working conditions
dc.subjectSolid-phase extraction
dc.subjectAcetone
dc.subjectAtomic absorption spectrometry
dc.subjectNitrogen compounds
dc.subjectOres
dc.subjectPalladium
dc.subjectResins
dc.subjectPalladium compounds
dc.titleSeparation and pre-concentration of palladium(II) from environmental and industrial samples by formation of a derivative of 1,2,4-triazole complex on Amberlite XAD-2010 resinen_US
dc.typeArticleen_US

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